Evaluation of nitrate quantification techniques for in-line analysis in drinking water

 

محفوظ في:
التفاصيل البيبلوغرافية
المؤلفون: Hernández-Alpízar, Laura, Coy-Herrera, Ricardo
التنسيق: artículo original
الحالة:Versión publicada
تاريخ النشر:2015
الوصف:The potential of four analytical methods for the quantification of nitrate is determined to be used in a continuous sampling set up: ion chromatography and the ultraviolet spectrophotometric screening, both in their benchtop version, Cadmium reduction with post-reaction and visible light absorption measurement and the direct ultraviolet spectrophotometric absorption screening but using mini-spectrophotometers and in flow injection of the sample and analysis (FIA) techniques. Accessories, toxicity of the reaction products, response, detection and quantification limits, linearity in the range of interest and sensitivity are considered for the evaluation. The direct measurement of ultraviolet absorption with flow injection was the best of the evaluated techniques. It has a linear response in the 0-10 mg/L range, WHO recommended range for drinking water, low reagents and accessories consuming, LOD 0,002 mg/L, LOQ 0,006 mg/L, and good sensitivity in the investigated range, meeting the required characteristics for in-line monitoring systems. 
البلد:Portal de Revistas TEC
المؤسسة:Instituto Tecnológico de Costa Rica
Repositorio:Portal de Revistas TEC
اللغة:Español
OAI Identifier:oai:ojs.pkp.sfu.ca:article/2446
الوصول للمادة أونلاين:https://revistas.tec.ac.cr/index.php/tec_marcha/article/view/2446
كلمة مفتاحية:Nitrate
in-line analysis
FIA
continuos sampling
spectrophotometry.
Nitratos
análisis en línea
muestreo continuo
espectrofotometría.