Determinación de ácidos grasos, glicerina libre y glicerina total en biodiésel

 

Αποθηκεύτηκε σε:
Λεπτομέρειες βιβλιογραφικής εγγραφής
Συγγραφείς: Fuentes Schweizer, Paola, Wong Monge, Anayansi
Μορφή: artículo original
Κατάσταση:Versión publicada
Ημερομηνία έκδοσης:2016
Περιγραφή:The validation of two analytical methods by gas chromatography was performed, in order to evaluate the quality of biodiesel (B100) and its usefulness as fuel. The performed methods were: determination of total content of fatty acid methyl esters (FAME) and determination of free and total glycerol content. Standards IN 14103: 2011 and ASTM D6584-13 were used as reference respectively. The performance parameters evaluated and documented for the two methods in the study were: linearity, detection limit and quantification limit, precision by repeatability and intermediate repeatability, truenes through a recovery test. Based on the evaluation of performance parameters and acceptance criteria it was concluded that the two methods are statistically and analytically under control; also both methods allow to establish a continuous assessment; demonstrating that the analytical procedures used are suitable for use as a routine screening test at CELEQ.
Χώρα:Portal de Revistas UCR
Ίδρυμα:Universidad de Costa Rica
Repositorio:Portal de Revistas UCR
Γλώσσα:Español
OAI Identifier:oai:portal.ucr.ac.cr:article/25391
Διαθέσιμο Online:https://revistas.ucr.ac.cr/index.php/cienciaytecnologia/article/view/25391
Λέξη-Κλειδί :biodiesel
fatty acid methyl esters (FAME)
free and total glycerin
gas chromatography
biodiésel
metil ésteres de ácidos grasos
glicerina libre y total
cromatografía de gases