Comparison between two chromatographic methods to determine chlorothalonil in a commercial fungicide

 

Tallennettuna:
Bibliografiset tiedot
Tekijät: Pérez López, Esteban, Rodríguez Rodríguez, Rosa Angélica
Aineistotyyppi: artículo original
Tila:Versión publicada
Julkaisupäivä:2019
Kuvaus:Introduction: Chlorothalonil can be determined by several analytical techniques, including gas chromatography (GC) and high performance liquid chromatography (HPLC). These two techniques are used often because they have a higher level of stability and sensitivity. Objective: To compare the efficacy of analytical methodologies by GC and by HPLC for the determination of chlorothalonil in a commercial fungicide. Methods: both the HPLC method and the GC method used by the laboratory were applied to equivalent samples and the results were compared with paired statistical tests. Results: both methods produced statistically equivalent and reliable results. These parameters were satisfactory: selectivity, range of work and linearity, limit of detection and quantification, repeatability, intermediate precision, robustness, veracity and bias; we consider them linear, precise and exact methods that meet the norms of the Costa Rican Accreditation Entity (ECA). Conclusions: both methods for determining chlorothalonil can be used reliably under the defined conditions.
Maa:Portal de Revistas UNED
Organisaatio:Universidad Estatal a Distancia
Repositorio:Portal de Revistas UNED
Kieli:Español
OAI Identifier:oai:revistas.investiga.uned.ac.cr:article/2627
Linkit:https://revistas.uned.ac.cr/index.php/cuadernos/article/view/2627
Sanahaku:agrochemicals
chlorothalonil
pesticides
analytical method
validation
agroquímicos
clorotalonil
plaguicidas
método analítico
validación