Validation of an analytical method with modified acid purity and iron matrices to measure heavy metals (Cd, Pb, Cr and As) in fertilizers
সংরক্ষণ করুন:
| লেখক: | , |
|---|---|
| বিন্যাস: | artículo original |
| বর্তমান অবস্থা: | Versión publicada |
| প্রকাশনার তারিখ: | 2022 |
| বিবরন: | Introduction: The frequent use of fertilizers in the Costa Rican agricultural sector causes environmental pollution; and heavy metals are among the main pollutants because of their high toxicity, strengthening the need for affordable and reliable local methods to assess pollution levels. Objective: To validate an adaptation of a method that uses modified acid purity and iron matrices to measure heavy metals (Cd, Pb, Cr and As) in fertilizers. Method: We tested four duplicate analyzes of a sample of known concentration with reactive grade acids and ultra-pure acids. For the iron interference test, we used eight replicates. We also did tests for bias, precision, detection limits, quantification limit, specificity, recovery, false positives and false negatives. Results: The new method proved satisfactory and its efficiency held by analytical performance parameters. Conclusions: The method is resistant to changes in acid purity, and tolerates matrices with iron concentrations under 5% m/m. |
| দেশ: | Portal de Revistas UNED |
| প্রতিষ্ঠান: | Universidad Estatal a Distancia |
| Repositorio: | Portal de Revistas UNED |
| ভাষা: | Español |
| OAI Identifier: | oai:revistas.investiga.uned.ac.cr:article/3485 |
| অনলাইন ব্যবহার করুন: | https://revistas.uned.ac.cr/index.php/cuadernos/article/view/3485 |
| মুখ্য শব্দ: | heavy metals fertilizer agrochemicals validation ICP metales pesados fertilizante agroquímicos validación |