Palladium-Catalyzed One-Pot Conversion of Aldehydes and Ketones into 4‑Substituted Homopropargyl Alcohols and 5‑En-3-yn-1-ols

 

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Detaylı Bibliyografya
Yazarlar: Umaña, Christian A., Cabezas Pizarro, Jorge A.
Materyal Türü: artículo original
Yayın Tarihi:2017
Diğer Bilgiler:Sequential treatment of 2,3-dichloropropene with magnesium and n-BuLi generated the equivalent of 1,3- dilithiopropyne, which adds regiospecifically to aldehydes and ketones to produce homopropargyl alcohols. The lithium acetylide intermediate formed in this protocol can be further reacted with aromatic and vinyl halides, under palladium catalysis, to produce 4-substituted homopropargyl alcohols and 5-en-3-yn-1-ols, respectively, in one-pot with good overall yields.
Ülke:Kérwá
Kurum:Universidad de Costa Rica
Repositorio:Kérwá
Dil:Inglés
OAI Identifier:oai:kerwa.ucr.ac.cr:10669/87985
Online Erişim:https://pubs.acs.org/doi/10.1021/acs.joc.7b01529
https://hdl.handle.net/10669/87985
Anahtar Kelime:Alcohols
Allenes
Aromatic compounds
Hydrocarbons
Palladium